I have separated your mixture of naphthalene, benzoic acid and p-tert-butylphenol. The percent recovery of all three were 70.4%, 86.4%, and 98.4%, respectively. Naphthalene was found to be impure, whereas benzoic acid and p-tert-butylphenol were found to be pure.
These chemicals were separated by the use of acid-base separation. The process began by adding 50mL of the sample and 50 mL of diethyl ether, a clear liquid, to a separatory funnel. The sample given began as a rocky solid with some…
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